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Jun 24, 2020 As the anode dissolves, phosphorous is exposed and the black film thickens. Eventually, as the anode shrinks and falls lower in the anode basket, the black film sloughs off and settles to the bottom of the anode bag. This is the so-called anode sludge. The sludge will also contain impurity elements not soluble in the acid-copper electrolyte.
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